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1Novel acetylene complexes of titanocene and permethyltitanocene without additional ligands. Synthesis spectral characteristics and X-ray diffraction study

V.V. Burlakov,A.V. Polyakov,A.I. Yanovsky,Yu.T. Struchkov,V.B. Shur,M.E. Vol'pin,U. Rosenthal,H. Görls

New acetylene complexes of titanocene and permethyltitanocene Cp2Ti(R1C2R2) and Cp2*Ti(R1C2R2) (R1R2SiMe3; R1Ph, R2SiMe3) without additional ligands have been prepared by the reaction of Cp2TiCl2 and Cp2*TiCl2 with equimolar amounts of Mg and the appropriate acetylene R1C2R2 in THF. The complexes have been isolated from the reaction mixture in an analytically pure state and characterized by spectral methods. The structures of complexes Cp2Ti(PhC2SiMe3), Cp2*Ti(PhC2SiMe3) and Cp2*Ti(Me3SiC2SiMe3) have been proved by an X-ray diffraction study. Some chemical properties of the synthesized complexes have been investigated.

1994Journal of Organometallic Chemistry（1994）引用：194

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2Synthesis, Structure, and Certain Transformations of S-(o-carboran-9-yl) Diphenylthiophosphinite

V. P. Balema,E. G. Rys,N. N. Godovikov,A. V. Polyakov,Yu. T. Struchkov

S-(o-Carboran-9-yl) diphenylthiophosphinite was obtained for the first time, and its structure and transformations were studied. A series of esters of thio- dithio-and selenothiophosphinic acids have been synthesized and complexes of tungsten and manganese were obtained containing the carboranylthiophosphinite ligand.

1992Bulletin of the Russian Academy of Sciences, Division of chemical science（1992）引用：2

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3Nucleophilic-Substitution in Allyl System of Codeine and Pseudocodeine - Crystalline and Molecular-Structure of 8-Beta-bis (Methoxycarbonyl)-Methyl-8-deoxypseudocodeine

VN KALININ,SA KAZANTSEVA,VV KOBAK,PV PETROVSKII,AV POLYAKOV,AI YANOVSKII,YT STRUCHKOV

ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.

1992ZHURNAL ORGANICHESKOI KHIMII（1992）引用：23

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4ChemInform Abstract: Molecular Structure and Distribution of Electron Density in 9‐azido‐m‐ Carborane at 160K

M. YU. ANTIPIN,A. V. POLYAKOV,V. G. TSIREL'SON, M. KAPPKHAN,V. V. GRUSHIN,YU. T. STRUCHKOV

AbstractChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.

1991ChemInform（1991）

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5ChemInform Abstract: Crystal and Molecular Structure of (η2‐acetylenedimethyldicarboxylate)bis(triphenylphosphane)nickel(0), (ph3p)2ni(meooccccoome); Influence of Metals on Acetylene Complexation

U. ROSENTHAL,G. OEHME,H. + GOERLS,V. V. BURLAKOV,A. V. POLYAKOV,A. I. YANOVSKY,YU. T. STRUCHKOV

ChemInformVolume 21, Issue 35 Physical Organic Chemistry ChemInform Abstract: Crystal and Molecular Structure of (η2-Acetylenedimethyldicarboxylate)bis(triphenylphosphane)nickel(0), (Ph3P)2Ni(MeOOCCCCOOMe); Influence of Metals on Acetylene Complexation U. ROSENTHAL, U. ROSENTHAL Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorG. OEHME, G. OEHME Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorH. + GOERLS, H. + GOERLS Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorV. V. BURLAKOV, V. V. BURLAKOV Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorA. V. POLYAKOV, A. V. POLYAKOV Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorA. I. YANOVSKY, A. I. YANOVSKY Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorYU. T. STRUCHKOV, YU. T. STRUCHKOV Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this author U. ROSENTHAL, U. ROSENTHAL Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorG. OEHME, G. OEHME Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorH. + GOERLS, H. + GOERLS Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorV. V. BURLAKOV, V. V. BURLAKOV Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorA. V. POLYAKOV, A. V. POLYAKOV Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorA. I. YANOVSKY, A. I. YANOVSKY Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this authorYU. T. STRUCHKOV, YU. T. STRUCHKOV Zentralinst. Org. Chem., Akad. Wiss. DDR, DDR-2500 RostockSearch for more papers by this author First published: August 28, 1990 https://doi.org/10.1002/chin.199035046Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat No abstract is available for this article. Volume21, Issue35August 28, 1990 RelatedInformation

1990ChemInform（1990）引用：13

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6SYNTHESIS AND ESTABLISHING OF STRUCTURE OF 2-(1-3-DIHYDRO-2-PHENYL-1,4-BENZODIOXINE-2-YL)-3-PHENYL-1,4-BENZODIOXINE

IB DZVINCHUK,AV POLYAKOV,MO LOZINSKY, YT STRUCHKOV

1990UKRAINSKII KHIMICHESKII ZHURNAL

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7THERMAL ORTHO-META-REARRANGEMENTS OF NICKEL CARBORANES - CRYSTAL AND MOLECULAR-STRUCTURE OF 3,1,2-BIPYNIC2B9H11 AND 2,1,7-BIPYNIC2B9H11

AA ERDMAN,ZP ZUBREICHUK,VP PROKOPOVICH,AV POLYAKOV,AI YANOVSKII,YT STRUCHKOV,NA MAIER,YA OLDEKOP

1989KOORDINATSIONNAYA KHIMIYA

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8NMR ANALYSIS OF ADDUCTS FROM ANTIPYRINE AND LANTHANIDE SHIFT-REAGENTS - MOLECULAR-STRUCTURE OF 2,3-DIMETHYL-1-PHENYL-5-ETHOXYPYRAZOLIUM BENZOSULFONATE

EI OBLAPENKO,AV POLYAKOV,AI ERMAKOV,AI YANOVSKII, AV KRYLOV,VG VORONIN, YT STRUCHKOV

1989KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII（1989）

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9NMR Study of Antipyrine Adducts with Lanthanide Shift Reagents. Molecular Structure of 2,3-Dimethyl -1-phenyl- 5-Ethoxypyrazole

E. I. Oblapenko,A. V. Polyakov,A. I. Ermakov,A. I. Yanovskii, A. V. Krylov,V. G. Voronin,Yu. T. Struchkov

The complex formation of antipyrine with LSR in CCl4 is studied. Recommendations for producing the limiting lanthanide induced shifts characteristic of the 1∶1 complex are given and the geometry of the complex formed is determined. Results of an x-ray structure study of the adduct which is formed upon reaction of antipyrine and the ethyl ester of benzenesulfonic acid are presented.

1989Chemistry of Heterocyclic Compounds（1989）

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10MOLECULAR AND CRYSTALLINE-STRUCTURE OF RUTHENIUM(II) CHLORODICARBONYL(1-DIPHENYLPHOSPHINOMETHYL-ORTHO-CARBORANE-P)(1-DIPHENYLPHOSPHINOMETHYL-ORTHO-CARBORANYL-B-3(6),P)