Non-invasive continuous health monitoring has become feasible with the advancement of biosensors. While monitoring certain biomarkers such as heart rate or skin temperature are now at a certain maturity, monitoring molecular biomarkers is still challenging. Progress has been shown in sampling, measurement, and interpretation of data toward non-invasive molecular sensors that can be integrated into daily wearable items. Toward this goal, this paper explores the potential of embroidered interdigitated transducer (IDT)-based sensors for non-invasive, continuous monitoring of human biomarkers, particularly glucose levels, in human sweat. The study employs innovative embroidery techniques to create flexible fabric-based sensors with gold-coated IDTs. In controlled experiments, we have shown the variation of glucose concentration in water can be wirelessly detected by tracking the resonant frequency of the embroidered sensors. The current sensors operate at 1.8 GHz to 2 GHz and respond to the change in glucose concentration with a sensitivity of 0.17 MHz/(mg/dL). The embroidered IDT-based sensors with wireless sensing will be a new measurement modality for molecular wearable sensors. The establishment of a wireless sensing mechanism for embroidered IDT-based sensors will be followed by an investigation of sweat for molecular detection. This will require adding functionalities for sampling and interpretation of acquired data. We envisage the embroidered IDT-based sensors offer a unique approach for seamless integration into clothing, paving the way for personalised, continuous health data capture.

The critical need for accurate and non-invasive temperature monitoring is prevalent in extreme environments, such as scuba diving. Current temperature measurement technologies present limitations, prompting the development of innovative solutions. We propose the integration of embroidered wearable thermocouple sensors, demonstrating their versatility and reliability in real-time temperature monitoring. T-type thermocouples, embroidered onto fabric, offer flexibility in sensor placement, eliminating the need for skin attachment. The results indicate efficient temperature detection across different body areas, from 32.5 °C at extremities to 37.5 °C at the axial position. Testing in scuba diving conditions reveals potential applications, including overheating alerts and hypothermia prevention. This technology bridges the gap between temperature measurement and the challenges of underwater exploration, enhancing diver safety and data collection capabilities.

The rapid growth of the global wearable technologies market is projected to reach $61.30 billion by 2030 which reflects a shift towards personalised health monitoring embedded in everyday activities. This paper explores the potential of embroidered interdigitated transducer (IDT)-based sensors for non-invasive, continuous monitoring of human biomarkers, particularly glucose levels, in human sweat. The study employs innovative embroidery techniques to create flexible fabric-based sensors with gold-coated IDTs. Experimental results demonstrate the sensor’s capability to detect water droplets and glucose concentrations, showcasing promising applications for health monitoring. The embroidered IDT-based sensors offer a unique approach for seamless integration into clothing, paving the way for personalised, continuous health data capture.

Anthropometric data form the cornerstone of garment pattern-making. This article introduces an artificial intelligence-driven approach, employing a back-propagation artificial neural network (BP-ANN), to predict the anthropometric data essential for crafting patterns for women's upper tops. The model adeptly processes minimal critical data from women's upper bodies, yielding projected dimensions that are arduous to manually measure yet crucial for tailoring body-fitting tops. Utilising a three-dimensional body scanner for accurate anthropometric data collection from 196 women in Sichuan Province, China, our study compares the BP-ANN model with a Linear Regression (LR) model. Results demonstrate superior predictive accuracy for BP-ANN. Notably, the BP-ANN model excels in efficiency and accuracy, particularly in challenging anthropometric parameters. The findings underscore the transformative potential of AI-based models in optimizing garment production processes, offering a precise alternative to traditional methods. This research contributes valuable insights for the integration of AI technology in advancing pattern-making practices.

The fabrication of metal–insulator– metal (MIM) diode using an ultrathin Al2O3 insulator layer, deposited using atomic layer deposition (ALD) is presented. The Al2O3 insulating layer was found to be highly uniform throughout the diode junction, effectively overcoming the main fabrication challenge in MIM diodes. The diodes exhibit strong non-linear current–voltage curves, have a typical zero-bias curvature coefficient of 5.4 V−1 and a zero-bias resistance of approximately 118 kΩ, a value considerably smaller than other MIM diode topologies and that allows more current to be rectified. Other results including current ratio and yield of the diode also competes favorably with the state-of-the-art MIM diodes such as the recently produced metal-octadecyltrichlorosilane (OTS)-metal structure.

A simple and elegant impedance-matching method for rectenna operating in a narrow frequency range is presented. The method used two coplanar strip lines emerging from the antenna feed-point, to correct for the reactive component of the antenna impedance on one side, and to connect the rectifier and transform its impedance on the other side. The experimental results were supported by numerical simulations, which suggest that the same impedance matching technique can be used for mm-waves and terahertz (THz) radiation applications. Microwave characterization of the fabricated devices (impedance-matched and non-matched) showed that the responsivity of the impedance-matched rectenna is approaching an order of magnitude higher at 20 GHz than that of a control device without a matching network.

Embroidery has been recently introduced as a new method to realize sensors especially for wearables.In this paper, we present a slot-loaded embroidered patch antenna to provide a simplified setup which allows the antenna to act as a stand-alone resonator.The design procedure, simulation, and implementation of an embroidered sensor are presented and discussed.It is demonstrated that this structure can be used without any need for external antennas as a wireless sensor.To demonstrate the feasibility of this technique, the design process using a slot-loaded antenna to achieve a high Q antenna, fabricated on an FR4 substrate, is presented and discussed.This structure is then manufactured, with practical results shown to agree with simulated results.Using this as a basis for subsequent designs, an embroidered slot-loaded patch is presented and discussed.We demonstrate this capability in an experiment where a set of solvents inside plastic bottles were interrogated using the embroidered antennas.

Although wearables have shown utility in many clinical-based studies, their transition to daily use is limited by their design-induced lack of integration to everyday clothing items. This chapter explores current flexible substrate sensors and their substrates, which have the potential to be developed into wearable items. We also discuss the barriers to entry for wearables in the fashion industry and how the gap between clothing and healthcare can and needs to be narrowed to facilitate widespread ease of use.

Temperature control within a microreactor is critical for biochemical and biomedical applications. Recently acoustothermal heating using surface acoustic wave (SAW) devices made of bulk LiNbO3 substrates have been demonstrated. However, these are generally fragile and difficult to be integrated into a single lab-on-a-chip. In this paper, we propose a rapid and controllable acoustothermal microheater using AlN/Si thin film SAWs. The device's acoustothermal heating characteristics have been investigated and are superior to other types of thin film SAW devices (e.g., ZnO/Al and ZnO/Si). The dynamic heating processes of the AlN/Si SAW device for both the sessile droplet and liquid within a polydimethylsiloxane (PDMS) microchamber were characterized. Results show that for the sessile droplet heating, the temperature at a high RF power is unstable due to significant droplet deformation and vibration, whereas for the liquid within the microchamber, the temperature can be precisely controlled by the input power with good stability and repeatability. In addition, an improved temperature uniformity using the standing SAW heating was demonstrated as compared to that of the travelling SAWs. Our work shows that the AlN/Si thin film SAWs have a great potential for applications in microfluidic heating such as accelerating biochemical reactions and DNA amplification. (C) 2020 Elsevier B.V. All rights reserved.

In this paper, we explore the acoustofluidic performance of zinc oxide (ZnO) thin-film surface acoustic wave (SAW) devices fabricated on flexible and bendable thin aluminum (Al) foils/sheets with thicknesses from 50 to 1500 μm. Directional transport of fluids along these flexible/bendable surfaces offers potential applications for the next generation of microfluidic systems, wearable biosensors and soft robotic control. Theoretical calculations indicate that bending under strain levels up to 3000 με causes a small frequency shift and amplitude change (<0.3%) without degrading the acoustofluidic performance. Through systematic investigation of the effects of the Al sheet thickness on the microfluidic actuation performance for the bent devices, we identify the optimum thickness range to both maintain efficient microfluidic actuation and enable significant deformation of the substrate, providing a guide to design such devices. Finally, we demonstrate efficient liquid transportation across a wide range of substrate geometries including inclined, curved, vertical, inverted, and lateral positioned surfaces using a 200 μm thick Al sheet SAW device.

Integration of microfluidics and biosensing functionalities on a single device holds promise in continuous health monitoring and disease diagnosis for point-of-care applications. However, the required functions of fluid handling and biomolecular sensing usually arise from different actuation mechanisms. In this work, we demonstrate that a single acoustofluidic device, based on a flexible thin film platform, is able to generate hybrid wave modes, which can be used for fluidic actuation (Lamb waves) and biosensing (thickness shear waves). On this integrated platform, we show multiple and sequential functions of mixing, transport and disposal of liquid volumes using Lamb waves, whilst the thickness bulk shear waves allow us to sense the chemotherapeutic Imatinib, using an aptamer-based strategy, as would be required for therapy monitoring. Upon binding, the conformation of the aptamer results in a change in coupled mass, which has been detected. This platform architecture has the potential to generate a wide range of simple sample-to-answer biosensing acoustofluidic devices.

In this paper, we report an embroidered rectangular split-ring resonator (SRR) operating at S band for material characterization based on the differences in dielectric parameters. We designed, fabricated and characterized SRR sensors on a conventional fabric that can be conformally attached over the surface of samples under investigation. The structures are made of conductive threads and can be embroidered on any dielectric fabric at low cost using conventional embroidery methods. We have demonstrated material characterization capability of the sensors using a specific design with a length of 60 mm and a width of 30 mm. We wrapped the sensors on low-density polyethylene (LDPE) bottles filled with deionized (DI) water and common solvents (ethanol, methanol, isopropanol and acetone) in our experiments. We measured the nominal resonant frequency of a specific sensor wrapped around an empty bottle as 2.07 GHz. The shifts in resonant frequencies when the bottle was filled with the solvents follow the dielectric constants of the solvents.

The Leidenfrost effect allows droplets to be transported on a virtually frictionless layer of vapor above a superheated substrate. The substrates are normally topographically structured using subtractive techniques to produce saw-tooth, herringbone, and other patterns and bulk heated, leading to significant challenges in energy consumption and controlled operation. Here, we propose a planar lithographic approach to levitate and propel droplets using temperature profiles, which can be spatially patterned and controlled in time. We show that micro-patterned electrodes can be heated and provide control of the pressure profile and the vapor flow. Using these almost featureless planar substrates, we achieve self-directed motion of droplets, with velocities of approximately 30 mms−1, without topographically structuring the substrate or introducing physical walls. Our approach has the potential to be integrated into applications, such as digital microfluidics, where frictionless and contactless droplet transport may be advantageous.

The conduction mechanisms in metal-insulator-metal junctions where the insulator consists of a self-assembled monolayer are investigated. Temperature dependence measurements from 2.5 to 300 K, show that the conduction is dominated by tunnelling only for temperatures below 20 K, while at higher temperatures surface-limited and bulk-limited mechanisms are observed. The experimental results are explained using a combination of direct (Simmons) tunnelling, Schottky emission, and Poole-Frenkel theory. Further insight is gained through numerical simulations based on the non-equilibrium Green-function formalism.

A fundamental limitation to the ability to transport sessile droplets is frictional forces arising from surface adhesion. This can be overcome by using the Leidenfrost effect on a heated substrate to levitate the droplet on a cushion of vapor. By structuring the surface under the droplet, the flow of vapor below the droplet can be controlled and this can be used to induce preferential droplet propulsion in a particular direction. However, while propulsion can be induced, the dramatic reduction in frictional forces leads to instability and it is difficult to control droplet motion when transporting droplets along a defined path. Here, we present a self-propulsion and self-centering concept using the principles of negative feedback to enable a droplet to be transported along a defined path. In our implementation, we use a combined herringbone and ratchet design, which provides the ability to control droplet position without compromising on speed. This intrinsic self-centering and correction via negative feedback offers the potential to design paths and tracks for droplets to follow, without the need for walls.

Often wetting is considered from the perspective of a single surface of a rigid substrate and its topographical properties such as roughness or texture. However, many substrates, such as membranes and meshes, have two useful surfaces. Such flexible substrates also offer the potential to be formed into structures with either a double-sided surface (e.g. by joining the ends of a mesh as a tape) or a single-sided surface (e.g. by ends with a half-twist). When a substrate possesses holes, it is also possible to consider how the spaces in the substrate may be connected or disconnected. This combination of flexibility, holes and connectedness can therefore be used to introduce topological concepts, which are distinct from simple topography. Here, we present a method to create a Slippery Liquid-Infused Porous Surface (SLIPS) coating on flexible conformable doubled-sided meshes and for coating complex geometries. By considering the flexibility and connectedness of a mesh with the surface properties of SLIPS, we show it is possible to create double-sided SLIPS materials with high droplet mobility and droplet control on both faces. We also exemplify the importance of flexibility using a mesh-based SLIPS pipe capable of withstanding laminar and turbulent flows for 180 and 90 minutes, respectively. Finally, we discuss how ideas of topology introduced by the SLIPS mesh might be extended to create completely new types of SLIPS systems, such as Mobius strips and auxetic metamaterials.

Much of the inspiration for the creation of superhydrophobic surfaces has come from nature, from plants such as the sacred lotus (Nelumbo nucifera), where the micro-scale papillae epidermal cells on the surfaces of the leaves are covered with nano-scale epicuticular wax crystalloids. The combination of the surface roughness and the hydrophobic wax coating produces a superhydrophobic wetting state on the leaves, allowing them to self-clean and easily shed water. Here, a simple scaled-up carbon nanoparticle spray coating is presented that mimics the surface of sacred lotus leaves and can be applied to a wide variety of materials, complex structures, and flexible substrates, rendering them superhydrophobic, with contact angles above 160°. The sprayable mixture is produced by combining toluene, polydimethylsiloxane, and inherently hydrophobic rapeseed soot. The ability to spray the superhydrophobic coating allows for the hydrophobisation of complex structures such as metallic meshes, which allows for the production of flexible porous superhydrophobic materials that, when formed into U-shaped channels, can be used to direct flows. The porous meshes, whilst being superhydrophobic, are also oleophilic. Being both superhydrophobic and oleophilic allows oil to pass through the mesh, whilst water remains on the surface. The meshes were tested for their ability to separate mixtures of oil and water in flow conditions. When silicone oil/water mixtures were passed over the meshes, all meshes tested were capable of separating more than 93% of the oil from the mixture.

Even with the recent extensive study into superhydrophobic surfaces, the fabrication of such surfaces on the inside walls of a pipe remains challenging. In this work we report a convenient bi-layered pipe design using a thin superhydrophobic metallic mesh formed into a tube, supported inside another pipe. A flow system was constructed to test the fabricated bi-layer pipeline, which allowed for different constant flow rates of water to be passed through the pipe, whilst the differential pressure was measured, from which the drag coefficient (ƒ) and Reynolds numbers (Re) were calculated. Expected values of ƒ were found for smooth glass pipes for the Reynolds number (Re) range 750–10 000, in both the laminar and part of the turbulent regimes. Flow through plain meshes without the superhydrophobic coating were also measured over a similar range (750  <  Re  <  14 000). After applying the superhydrophobic coating, ƒ was found for 4000  <  Re  <  14 000 and was found to be less than that of an uncoated mesh, but greater than that of a smooth glass pipe of the same diameter. This demonstrates that a superhydrophobic mesh can support a plastron and provide a drag reduction compared to a plain mesh, however, the plastron is progressively destroyed with use and in particular at higher flow rates.

An energy saving Leidenfrost levitation method is introduced to transport microdroplets with virtually frictionless contact between the liquid and solid substrate. Through microengineering of the heating units, selective areas of the whole substrate can be electrothermally activated. A droplet can be levitated as a result of the Leidenfrost effect and further transported when the substrate is tilted slightly. Selective electroheating produces a uniform temperature distribution on the heating units within 1 s in response to a triggering voltage. Alongside these experimental observations, finite element simulations were conducted to understand the role of substrate thermal conductivity on the temperature profile of the selectively heated substrate. We also generated phase diagrams to verify the Leidenfrost regime for different substrate materials. Finally, we demonstrated the possibility of controlling low friction high speed droplet transportation (∼65 mm/s) when the substrate is tilted (∼7°) by structurally designing the substrate. This work establishes the basis for an entirely new approach to droplet microfluidics.

An effective impedance matching technique for rectennas (an antenna coupled with rectifier) operating at specific frequencies is presented. The rectifier consists of a MIM junction with a molecular insulator. The method used two coplanar strip lines emerging from the antenna feed-point, to correct for the reactive component of the antenna impedance on one side, and to connect the rectifier and transform its impedance on the other side. Microwave and mm-wave characterization of the devices showed that the output voltage of the impedance matched rectenna is almost an order of magnitude higher than that of a control device without matching network at 20 GHz.