A simple and efficient one-pot synthesis of alkyl 2-(alkyl)-4-methyl-2-thioxo-2,3-dihydrothiazole-5-carboxylates from the reaction of primary alkylamines and carbon disulfide in the presence of 2-chloro-1,3-dicarbonyl compounds is described. This new protocol has several advantages such as lack of necessity of the catalyst, good yields, mild conditions and short times for reaction.
A simple and efficient one-pot synthesis of 1-[3-alkyl-4-methyl-2-thioxo-2,3-dihydrothiazole-5-yl]-ethanones from the reaction of primary alkylamines and carbon disulfide in the presence of 3-chloro acetylacetone is described. This protocol has several advantages such as lack of need for a solvent and catalyst, high yields, mild conditions and short reaction times.
Nasir Iravani合作论文数Chemistry Department, Islamic Azad University2
marzieh khadamati合作论文数1somaieh varnaseri合作论文数1
M.M. Monfared合作论文数Department of Mechanical Engineering, Islamic Azad University1Jalal Albadi合作论文数Behbahan Khatam Alanbia University of Technology1
Bahador Karami合作论文数Department of Chemistry;Yasouj University;Department of Chemistry, Yasouj University1
