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1ChemInform Abstract: Reaction of Vinylpyridines with Active Modifications of Elemental Phosphorus in KOH/DMSO.

N. K. Gusarova,S. I. Shaikhudinova,T. I. Kazantseva,B. G. Sukhov,V. I. Dmitriev,L. M. Sinegovskaya,Yu. V. Smetannikov,N. P. Tarasova,B. A. Trofimov

2010Cheminform（2010）引用：3

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2Reaction of Vinylpyridines with Active Modifications of Elemental Phosphorus in KOH/DMSO

N. K. Gusarova,S. I. Shaikhudinova,T. I. Kazantseva,B. G. Sukhov,V. I. Dmitriev,L. M. Sinegovskaya,Yu. V. Smetannikov,N. P. Tarasova,B. A. Trofimov

The phosphorylation of 2-vinyl- and 4-vinylpyridines by white phosphorus and active modifications of red phosphorus (obtained by thermal polymerization of white phosphorus in the presence of graphite or the action of ionizing radiation in benzene) in the KOH/DMSO superbase system at room temperature leads to the formation of tris[2-(2-pyridyl)ethyl]- and tris[2-(4-pyridyl)ethyl]phosphine oxides in 58-72% yield. These oxides are promising ligands for design of metal complex catalysts. These vinylpyridines react less efficiently with ordinary red phosphorus and the yield of the corresponding tris(2-pyridylethyl)phosphine oxides does not exceed 10%.

2002ChemInform（2002）引用：14

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3Reactions of Elemental Phosphorus and Phosphine with Electrophiles in Superbasic Systems: XIV.1 Phosphorylation of 2-Vinylnaphthalene with Elemental Phosphorus and Phosphines in the KOH-DMSO System

N. K. Gusarova,S. I. Shaikhutdinova,T. I. Kazantseva,S. F. Malysheva,B. G. Sukhov,N. A. Belogorlova,V. I. Dmitriev,B. A. Trofimov

Elemental phosphorus (red or white) reacts with 2-vinylnaphthalene while heating at 90-96°C in the superbasic KOH-DMSO system to form 2-(2-naphthyl)ethylphosphine, 2-(2-naphthyl)ethylphosphinic acid, bis[2-(2-naphthyl)ethyl]phosphine, bis[2-(2-naphthyl)ethyl]phosphine oxide, and tris[2-(2-naphthyl)ethyl]phosphine oxide in a total yield of up to 40%. Selective conditions for preparing the tertiary phosphine oxide from white phosphorus and 2-vinylnaphthalene in 58% yield were found. Phosphine and (2-phenylpropyl)phosphine add to 2-vinylnaphthalene in the KOH-DMSO system to form, under certain conditions, corresponding secondary phosphines in high yields.

2002Russian Journal of General Chemistry（2002）引用：26

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4Reactions of Elemental Phosphorus and Phosphine with Electrophiles in Superbasic Media: XI.1 Phosphorylation of 4-Methoxybenzyl Chloride with Elemental Phosphorus and Phosphine

S. I. Shaikhutdinova,T. I. Kazantseva,N. K. Gusarova,V. I. Dmitriev,B. A. Trofimov

4-Methoxybenzyl chloride reacts with elemental (red or white) phosphorus under the conditions of phase-transfer catalysis (concentrated aqueous KOH, dioxane, benzyltriethylammonium chloride, 85-90°C, argon) to give as major product tris(4-methoxybenzyl)phosphine oxide in up to 45% yield. With white phosphorus at lower (70°C) temperature this reaction yields mainly bis(4-methoxybenzyl)phosphine oxide. Phosphine reacts with 4-methoxybenzyl chloride in superbasic KOH-DMSO suspension, and under definite conditions bis(4-methoxybenzyl)phosphine oxide is predominantly formed.

2001Russian Journal of General Chemistry（2001）引用：4

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5Reactions of red phosphorus and phosphine with electrophiles in superbasicsystems. ix. addition of phosphine to vinylpyridines in the koh-dmso system

Gusarova Nina K,Trofimov Boris A,Svetlana F. Malysheva,S. I. Shaikhudinova,Natal’ya A. Belogorlova,Svetlana N. Arbuzova,K. V. Nepomnyashchikh,V. I. Dmitriev

1997Russian Journal of General Chemistry（1997）引用：3

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6Reactions of red phosphorus and phosphine with electrophiles in superbasic systems .9. Attachment of phosphine to vinylpyridines in KOH-DMSO system

N. K. Gusarova,B. A. Trofimov,S. F. Malysheva,S. I. Shaikhudinova,N. A. Belogorlova,S. N. Arbuzova,K. V. Nepomnyashchikh,V. I. Dmitriev

1997ZHURNAL OBSHCHEI KHIMII（1997）引用：23

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7SYNTHESIS OF DIBENZYLPHOSPHINOUS ACID FROM PHOSPHINE AND BENZYL CHLORIDE

S. I. Shaikhudinova,V. I. Dmitriev,K. V. Nepomnyashchikh,N. K. Gusarova,B. A. Trofimov

1997ZHURNAL OBSHCHEI KHIMII（1997）引用：23

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8SYNTHESIS AND ANTIBACTERIAL ACTIVITY OF TRIS{2-I4-(I-BEN ZYLPYRIDINIO)IET HYL}- PHOSPHINOXIDE TRICHLORIDE

Nina K Gusarova,E E Kuznetsova,S I Shaikhudinova,V I Dmitriev,Svetlana F Malysheva,G V Kozlova,Boris A Trofimov

1996Pharmaceutical Chemistry Journal引用：23

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9ChemInform Abstract: Synthesis and Antibacterial Activity of Tris(2‐(4‐(1‐benzylpyridinium)) Ethyl)phosphine Oxide Trichloride.

N. K. GUSAROVA,E. E. KUZNETSOVA,S. I. SHAIKHUDINOVA,V. I. DMITRIEV,S. F. MALYSHEVA,G. V. KOZLOVA,B. A. TROFIMOV

AbstractChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.

1996引用：1

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10Synthesis and Antibacterial Activity of Tris{2-[4-(1-benzylpyridinio)]ethyl}-phosphinoxide Trichloride

N. K. Gusarova,É. É. Kuznetsova,S. I. Shaikhudinova,V. I. Dmitriev,S. F. Malysheva,G. V. Kozlova,B. A. Trofimov

1996Pharmaceutical Chemistry Journal（1996）引用：2

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11REACTIONS OF RED PHOSPHORUS WITH ELECTROPHILES IN SUPERBASIC SYSTEMS. VII.SINGLE-STAGE SYNTHESIS OF PHOSPHOLANES AND PHOSPHORINANES FROM RED PHOSPHOR US AND ALPHA ,OMEGA -DIHALOALKANES

N. K. Gusarova,S. I. Shaikhudinova,V. I. Dmitriev,S. F. Malysheva,S. N. Arbuzova,B. A. Trofimov

1995Russian Journal of General Chemistry（1995）引用：23

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12ChemInform Abstract: Reactions of Red Phosphorus with Electrophiles in Superbasic Systems. Part 6. Identification of the Products of Phosphorylation of Phenylacetylene with the System P‐KOH‐HMPA under Conditions of Mechano‐ Chemical Activation.

N. K. GUSAROVA,S. N. ARBUZOVA,S. I. SHAIKHUDINOVA,S. F. MALYSHEVA,T. N. RAKHMATULINA,S. V. ZINCHENKO,V. I. DMITRIEV,B. A. TROFIMOV

1994ChemInform（1994）

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13REACTION OF RED PHOSPHORUS WITH ELECTROPHILES IN SUPERBASIC SYSTEMS .6. IDENTIFICATION OF PRODUCTS OF PHENYLACETYLENE PHOSPHORYLATION WITH P-KOH-HMPTA TRIAD UNDER MECHANIC-CHEMICAL ACTIVATION

NK GUSAROVA,SN ARBUZOVA,SI SHAIKHUDINOVA,SF MALYSHEVA,TN RAKHMATULINA,SV ZINCHENKO,VI DMITRIEV,BA TROFIMOV

1993ZHURNAL OBSHCHEI KHIMII

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14Synthesis of Tris(2,2-Dialkoxyethyl)phosphine Oxides from Red Phosphorus and 1,1-Dialkoxy-2-bromoethanes in Superbase Systems

B. A. Trofimov,N. K. Gusarova,S. I. Shaikhudinova,T. N. Rakhmatulina,S. F. Malysheva,L. A. Oparina,V. I. Dmitriev,M. G. Voronkov

1992ChemInform（1992）引用：2

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15Superbase-Induced Generation of Phosphide and Phosphinite Ions As Applied in Organic-Synthesis

BA TROFIMOV,NK GUSAROVA,SF MALYSHEVA,TN RAKHMATULINA,MG VORONKOV,VI DMITRIEV,SI SHAIKHUDINOVA

1991ChemInform（1991）引用：32

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16ChemInform Abstract: Phosphorylation of 4‐vinylpyridine with Elemental Phosphorus in the System KOH ‐ Dimethyl Sulfoxide.

B. A. TROFIMOV,V. I. DMITRIEV,T. I. KAZANTSEVA,S. I. SHAIKHUDINOVA,S. F. MALYSHEVA,M. V. SIGALOV,N. K. GUSAROVA

1991

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17Reaction Of Red Phosphorus With Electrophiles In Superbasic Systems .2. Synthesis Of Triorganylphosphinoxides From Red Phosphorus And Organylhalides

Nk Gusarova,Sf Malysheva,Tn Rakhmatulina,Vi Dmitriev,Si Shaikhudinova,Lm Sinegovskaya,Ba Trofimov

1990ZHURNAL OBSHCHEI KHIMII

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18Phosphorylation Of 4-Vinylpyridine By Element Phosphorus In The Koh-Dimethyl Sulfoxide System

Ba Trofimov,Vi Dmitriev, Ti Kazantseva,Si Shaikhudinova,Sf Malysheva,Mv Sigalov,Nk Gusarova

1990ZHURNAL OBSHCHEI KHIMII

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19ChemInform Abstract: Reaction of Red Phosphorus with Electrophiles in Superbasic Systems. Part 2. Synthesis of Triorganylphosphine Oxides from Red Phosphorus and Organyl Halides.

N. K. GUSAROVA,S. F. MALYSHEVA,T. N. RAKHMATULINA,V. I. DMITRIEV,S. I. SHAIKHUDINOVA,L. M. SINEGOVSKAYA,B. A. TROFIMOV

ChemInformVolume 21, Issue 51 Organoelement Compounds ChemInform Abstract: Reaction of Red Phosphorus with Electrophiles in Superbasic Systems. Part 2. Synthesis of Triorganylphosphine Oxides from Red Phosphorus and Organyl Halides. N. K. GUSAROVA, N. K. GUSAROVA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorS. F. MALYSHEVA, S. F. MALYSHEVA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorT. N. RAKHMATULINA, T. N. RAKHMATULINA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorV. I. DMITRIEV, V. I. DMITRIEV Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorS. I. SHAIKHUDINOVA, S. I. SHAIKHUDINOVA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorL. M. SINEGOVSKAYA, L. M. SINEGOVSKAYA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorB. A. TROFIMOV, B. A. TROFIMOV Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this author N. K. GUSAROVA, N. K. GUSAROVA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorS. F. MALYSHEVA, S. F. MALYSHEVA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorT. N. RAKHMATULINA, T. N. RAKHMATULINA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorV. I. DMITRIEV, V. I. DMITRIEV Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorS. I. SHAIKHUDINOVA, S. I. SHAIKHUDINOVA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorL. M. SINEGOVSKAYA, L. M. SINEGOVSKAYA Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this authorB. A. TROFIMOV, B. A. TROFIMOV Irkutsk. inst. org. khim. Sib. otd. AN SSSR, USSRSearch for more papers by this author First published: December 18, 1990 https://doi.org/10.1002/chin.199051242Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onEmailFacebookTwitterLinkedInRedditWechat No abstract is available for this article. References N. K. GUSAROVA, S. F. MALYSHEVA, T. N. RAKHMATULINA, V. I. DMITRIEV, S. I. SHAIKHUDINOVA, L. M. SINEGOVSKAYA, B. A. TROFIMOV, Reaction of Red Phosphorus with Electrophiles in Superbasic Systems. Part 2. Synthesis of Triorganylphosphine Oxides from Red Phosphorus and Organyl Halides., Zh. Obshch. Khim., 1990, 60(122), 828–832. Web of Science®Google Scholar Volume21, Issue51December 18, 1990 ReferencesRelatedInformation

1990ChemInform（1990）

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20ChemInform Abstract: Reaction of Red Phosphorus with Allyl Halides under Phase‐Transfer Catalysis.

Б. А. Трофимов,Svetlana F. Malysheva,Nina K. Gusarova,V. I. Dmitriev,S. I. Verkhoturova,T. N. Rakhmatulina,V. I. Donskikh, М. Г. Воронков

ChemInformVolume 21, Issue 14 Organoelement Compounds ChemInform Abstract: Reaction of Red Phosphorus with Allyl Halides Under Phase-Transfer Catalysis. B. A. TROFIMOV, B. A. TROFIMOV Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorS. F. MALYSHEVA, S. F. MALYSHEVA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorN. K. GUSAROVA, N. K. GUSAROVA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorV. I. DMITRIEV, V. I. DMITRIEV Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorS. I. SHAIKHUDINOVA, S. I. SHAIKHUDINOVA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorT. N. RAKHMATULINA, T. N. RAKHMATULINA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorV. I. DONSKIKH, V. I. DONSKIKH Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorM. G. VORONKOV, M. G. VORONKOV Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this author B. A. TROFIMOV, B. A. TROFIMOV Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorS. F. MALYSHEVA, S. F. MALYSHEVA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorN. K. GUSAROVA, N. K. GUSAROVA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorV. I. DMITRIEV, V. I. DMITRIEV Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorS. I. SHAIKHUDINOVA, S. I. SHAIKHUDINOVA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorT. N. RAKHMATULINA, T. N. RAKHMATULINA Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorV. I. DONSKIKH, V. I. DONSKIKH Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this authorM. G. VORONKOV, M. G. VORONKOV Irkutsk. inst. org. khim. Sib. otd. AN SSSRSearch for more papers by this author First published: April 3, 1990 https://doi.org/10.1002/chin.199014217Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat No abstract is available for this article. Volume21, Issue14April 3, 1990 RelatedInformation

1990ChemInform（1990）

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