目的 建立子宫锭的质量控制标准.方法 采用薄层色谱法对处方中的血竭、蛇床子进行定性鉴别研究;分别采用高效液相色谱法和气相色谱法对子宫锭中的儿茶素和麝香酮进行含量测定.结果 薄层色谱可检出血竭、蛇床子的特征斑点;儿茶素在0.632 5 ～1.265 0 μg范围呈良好的线性关系(r=0.999 9),平均回收率为98.71％,RSD=1.56％;麝香酮在0.134 4 ～0.302 4 μg范围呈良好的线性关系(r=0.999 8),平均回收率为98.36％,RSD=1.82％.结论 本方法准确、灵敏、重复性好,为子宫锭的质量控制提供了依据.

To understand the quality of abstracts of Traditional Chinese Medicine (TCM) papers,the author reviews the journals about TCM,and TCM combined with Western Medicine.Five kinds of flaws are identified,namely,lack of common sense,inconsistency,illogicality,missing key points,and not following relevant requirements.The major reason for such flaws is the weakness of editors,which can be further broken down to four kinds,lack of professionlism,knowledge,vocabulary,and familiarity with relevant requirements.Improvement could be made through enhancement of training and annual inspection.

以近现代上海气功的发展及其成果为线索,探讨沪上气功的主要特征。认为这些特征主要有:广纳百川、和而不同的气功功法,崇尚科学、敢为人先的气功科研,建"功"立业、教学为先的人才培养,著书立说、惠泽"功众"的人文气息等,并认为这是海上气功长盛不衰的源泉与动力。

<正>《儒门事亲》是元代著名医家张从正的著作,该书集中体现了他的学术思想和特色。张从正主张"驱邪存正"的治疗观点,认为治病先驱邪,邪去则元气自复,擅用汗、吐、下三法,为金元四大家之一,为中医学的发展作出了杰出的贡献。张从正提出"汗、下、吐,以若草木治病者也;补者,以谷、肉、果、菜养口体者也",认为谷、肉、果、菜犹如盛世中的德教,而汗、吐、下犹如乱世之中的刑罚。人在无病时用谷、肉、果、菜即可,而在生病时必须用汗、吐、下方能去之。张从正的汗、吐、下三法有着广泛的含义,除药物外,还包括针灸、心理、食疗、

目的建立祛湿散质量标准。方法采用显微鉴别法对制剂中黄芩、大黄进行显微鉴别;采用TLC法对制剂中青黛进行定性鉴别研究;采用HPLC法对黄芩的有效成分黄芩苷进行含量测定,选用Agilent Eclipse XDB-C18(150 mm×4.6 mm,5μm)色谱柱;甲醇-水-磷酸(47:53:0.2)为流动相,流速1.0 mL/min;柱温:室温;检测波长280 nm。结果黄芩、大黄的显微鉴别方法简捷、快速环保;青黛的薄层鉴别方法专属性强,空白无干扰。黄芩苷的加样回收率99.108%,n=5,RSD=1.0417%,黄芩苷在25.228μg/mL～111.0032μg/mL范围内呈良好的线性关系。结论该方法能够控制祛湿散的药品质量。

<正>白芷为伞形科植物白芷Angelica dahurica(Fisch.ex Hoffm.)Benth.et或杭白芷Angelica dahurica(Fisch.ex Hoffm.)Benth.et Hook.f.var.formosana(Boiss.)Shan et Yuan的干燥根。原名白茝,徐鏳云:"初生根干为芷,则白芷之义取乎此也。"入药首载于《神农本草经》[1],常用别名有香白芷、杭白芷、川白芷、会白芷、祁白芷、禹白芷、香大活,夏、秋间叶黄时采挖,除去须根及泥沙,晒干或低温干燥,以条粗壮、体重、粉性足、香气浓郁者为佳。其味辛,性温,归肺、脾、胃经,具有散风除湿,通窍止痛,消肿排脓的功能,用于

目的建立中药制剂颈椎康复丸质量标准。方法对制剂中甘草、黄芪进行显微鉴别研究;采用薄层色谱法对制剂中白芍、葛根进行定性鉴别研究。结果建立了颈椎康复丸的质量标准,包括甘草、黄芪的显微鉴别方法及白芍、葛根的薄层色谱鉴别方法。显微镜下观察可见甘草纤维、草酸钙方晶形成晶纤维、具缘纹孔导管、木栓细胞以及黄芪的纤维。选择中国药典方法进行4批次该制剂主要组成药物白芍、葛根的薄层层析鉴别,斑点显色清晰,分离效果好,阴性无干扰。结论本法简便迅速,重现性好,能较好地控制产品的质量,有利于医院制剂颈椎康复丸质量标准的提升。

Objective To set up the quality standard of Cervical Vertebra Rehabilitation Pill.Methods TLC were used to the qualitative identification of Red-rooted Salvia and Rhizoma Cyperi in the preparation.The content of peoniflorin,the effective component of Radix Paeoniae Alba in the preparation,was determined by HPLC,using Agilent Eclipse XDB-C18(150 mm×4.6 mm,5 μm) and acetonitrile-0.1% phosphoric acid solution(14∶86) as mobile phase with flow rate of 1.0 mL/min.The column temperature was room temperature,and the detection wavelength was 230 nm.Results The TLC method for Root of Red-rooted Salvia and Rhizoma Cyperi identification showed strong specificity and good repetitiveness.Peoniflorin presented a good linear relationship within the range of 0.202 884-1.014 42 μg,and the recovery rate was 98.79%,RSD was 0.865%(n=5).Conclusion These methods are useful for quality control and improvement of Cervical Vertebra Rehabilitation Pill.